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This book deals with experimental results of the physical characterization of several important dielectric materials of great current interest. The experimental tools used for the analysis of these materials include X-ray diffraction, dielectric measurements, magnetic measurements using a vibrating sample magnetometer, optical measurements using a UV-Visible spectrometer etc. Keywords: Materials Science, Dielectric Materials, Nanocrystalline NiO, GaO Powders, Multiferroic Material, ZnO Nanoparticles, ZnO Ceramics.